Search results for "single crystal XRD"

showing 2 items of 2 documents

Characterization of synthetic Fe-Mg silicate spinels in the gamma-(Mgx,Fe1-x)2SiO4 series by means of single crystal XRD (x=0,0.4,0.5)

2009

synthetic Fe-Mg silicate spinels gamma-(MgxFe1-x)2SiO4 series single crystal XRD
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Spectral and structural studies on Ni(II) dithiocarbamates: Nickel sulfide nanoparticles from a dithiocarbamate precursor

2015

Abstract Three new planar Ni(II) dithiocarbamate complexes; [Ni(4-dpmpzdtc)2] (1), [Ni(4-dpmpzdtc)(PPh3)(NCS)] (2) and [Ni(bupcbzdtc)(PPh3)(NCS)] (3) (where, 4-dpmpzdtc = 4-(diphenylmethyl)piperazinecarbodithioato anion, bupcbzdtc = N-butyl-N-(4-chlorobenzyl))dithiocarbamato anion and PPh3 = triphenylphosphine) with “NiS4” and “NiS2PN” chromophore units were synthesized and characterized by single crystal X-ray structural analysis as well as UV–Vis, IR and NMR (1H, 13C and 31P) spectroscopy. For 2, 1H–1H COSY spectrum was also recorded. Single crystal X-ray structural analysis of 1–3, reveals a slightly distorted square planar geometry in all three complexes wherein the steric and electroni…

Steric effectschemistry.chemical_classificationNickel sulfidesynthesisChemistrySolvothermal synthesisInorganic chemistryNanoparticlesingle crystal XRDChromophoreInorganic ChemistrydithiocarbamateCrystallographychemistry.chemical_compoundSEMTEMMaterials Chemistrynickel sulfidePhysical and Theoretical ChemistrySpectroscopyDithiocarbamateta116Single crystalInorganica Chimica Acta
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